Spektraris NMR
Tamulamides B
Common Name: Tamulamides B
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C34H43NO10/c1-19(37)35-18-32-21(38)14-27-31(43-32)17-34(2)33(44-27)16-30-26(45-34)12-11-25-29(42-30)15-28-24(40-25)10-9-22-23(41-28)8-7-20(39-22)6-4-3-5-13-36/h3-13,20-33,38H,14-18H2,1-2H3,(H,35,37)/b5-3+,6-4+/t20-,21-,22+,23-,24-,25+,26-,27+,28+,29-,30+,31-,32+,33-,34+/m1/s1
InChIKey: InChIKey=CPSGTWUSXJPPFV-WBUGLCRUSA-N
Formula: C34H43N1O10
Molecular Weight: 625.707265
Exact Mass: 625.288697
NMR Solvent: CD2Cl2
MHz:
Calibration:
NMR references: 13C - Truxal, L.T., Bourdelais, A.J., Jacocks, H., Abraham, W.M., Baden, D.G. J Nat Prod (2010) 73, 536-40
Species:
Notes: Family : Polyketides, Type : Polycyclic-ethers; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH3) | 23.1 |
| 2 (C) | 172.7 |
| 3 (CH2) | 40.6 |
| 4 (CH) | 82.4 |
| 5 (CH) | 65.4 |
| 6 (CH2) | 36.9 |
| 7 (CH) | 79 |
| 8 (CH) | 77.2 |
| 9 (CH2) | 43.5 |
| 10 (C) | 72.9 |
| 11 (CH) | 78.8 |
| 12 (CH2) | 32.5 |
| 13 (CH) | 79.6 |
| 14 (CH) | 73.1 |
| 15 (CH) | 133 |
| 16 (CH) | 131.5 |
| 17 (CH) | 80.4 |
| 18 (CH) | 77.5 |
| 19 (CH2) | 38.8 |
| 20 (CH) | 77.7 |
| 21 (CH) | 80.3 |
| 22 (CH) | 132.5 |
| 23 (CH) | 131.9 |
| 24 (CH) | 77.6 |
| 25 (CH) | 76.1 |
| 26 (CH) | 128.7 |
| 27 (CH) | 128.7 |
| 28 (CH) | 74.6 |
| 29 (CH) | 142.1 |
| 30 (CH) | 128.6 |
| 31 (CH) | 151 |
| 32 (CH) | 132.4 |
| 33 (CH) | 193.9 |
| 34 (CH3) | 15.7 |
