Spektraris NMR
Methyl 20(21)-dehydrolucidenate A
Common Name: Methyl 20(21)-dehydrolucidenate A
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C28H38O6/c1-15(8-9-22(33)34-7)16-12-21(32)28(6)24-17(29)13-19-25(2,3)20(31)10-11-26(19,4)23(24)18(30)14-27(16,28)5/h16-17,19,29H,1,8-14H2,2-7H3/t16-,17+,19+,26+,27-,28+/m1/s1
InChIKey: InChIKey=WISYORQOKQXQDW-LCTKWGEDSA-N
Formula: C28H38O6
Molecular Weight: 470.598783
Exact Mass: 470.266839
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Akihisa, T., Tagata, M., Ukiya, M., Tokuda, H., Suzuki, T., Kimura, Y. J Nat Prod (2005) 68, 559-63
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Lanostanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 36 |
| 2 (CH2) | 34.5 |
| 3 (C) | 215.9 |
| 4 (C) | 46.8 |
| 5 (CH) | 48.9 |
| 6 (CH2) | 29.1 |
| 7 (CH) | 65.7 |
| 8 (C) | 159.8 |
| 9 (C) | 140.9 |
| 10 (C) | 38.5 |
| 11 (C) | 198 |
| 12 (CH2) | 49.8 |
| 13 (C) | 45.5 |
| 14 (C) | 58.3 |
| 15 (C) | 215.5 |
| 16 (CH2) | 39.5 |
| 17 (CH) | 46.7 |
| 18 (CH3) | 19.3 |
| 19 (CH3) | 18.6 |
| 20 (C) | 145.8 |
| 21 (CH2) | 111.6 |
| 22 (CH2) | 31.8 |
| 23 (CH2) | 32.6 |
| 24 (C) | 173.2 |
| 28 (CH3) | 27 |
| 29 (CH3) | 20.9 |
| 30 (CH3) | 25.2 |
| 24a (CH3) | 51.5 |
