Spektraris NMR
20-Hydroxylucidenic acid P
Common Name: 20-Hydroxylucidenic acid P
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C29H42O9/c1-14(30)38-24-23(36)22-21(15(31)12-16-25(2,3)18(32)8-10-26(16,22)4)29(7)19(33)13-17(28(24,29)6)27(5,37)11-9-20(34)35/h15-18,24,31-32,37H,8-13H2,1-7H3,(H,34,35)/t15-,16-,17+,18-,24+,26-,27?,28-,29-/m0/s1
InChIKey: InChIKey=FFMHRFMHJKVBHE-OOLUJHIHSA-N
Formula: C29H42O9
Molecular Weight: 534.639497
Exact Mass: 534.282883
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Akihisa, T., Tagata, M., Ukiya, M., Tokuda, H., Suzuki, T., Kimura, Y. J Nat Prod (2005) 68, 559-63
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Lanostanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 34.4 |
| 2 (CH2) | 27.4 |
| 3 (CH) | 78.1 |
| 4 (C) | 38.6 |
| 5 (CH) | 49.1 |
| 6 (CH2) | 26.7 |
| 7 (CH) | 66.1 |
| 8 (C) | 155.9 |
| 9 (C) | 142.9 |
| 10 (C) | 38.6 |
| 11 (C) | 191 |
| 12 (CH) | 79.1 |
| 13 (C) | 49.8 |
| 14 (C) | 61 |
| 15 (C) | 214.5 |
| 16 (CH2) | 37.1 |
| 17 (CH) | 50.2 |
| 18 (CH3) | 14.2 |
| 19 (CH3) | 18.5 |
| 20 (C) | 86.7 |
| 21 (CH3) | 25.2 |
| 22 (CH2) | 34.6 |
| 23 (CH2) | 28.3 |
| 24 (C) | 175.5 |
| 28 (CH3) | 28.1 |
| 29 (CH3) | 15.4 |
| 30 (CH3) | 24.5 |
| 12a (C) | 170.3 |
| 12b (CH3) | 21.2 |
