Spektraris NMR
17-Dimethylaminolobohedleolide
Common Name: 17-Dimethylaminolobohedleolide
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C22H33NO4/c1-15-7-5-9-17(21(24)25)10-6-8-16(2)13-20-18(12-11-15)19(14-23(3)4)22(26)27-20/h7,10,13,18-20H,5-6,8-9,11-12,14H2,1-4H3,(H,24,25)/b15-7+,16-13+,17-10-/t18-,19-,20-/m0/s1
InChIKey: InChIKey=HRPBIJBOFQXOTL-JEJSWHNFSA-N
Formula: C22H33N1O4
Molecular Weight: 375.502597
Exact Mass: 375.240959
NMR Solvent: CD3OD
MHz:
Calibration:
NMR references: 13C - Rashid, M.A., Gustafson, K.R., Boyd, M.R. J Nat Prod (2000) 63, 531-3
Species:
Notes: Family : Terpenoids, Type : Diterpenoids, Group : Cembranes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH) | 44 |
| 2 (CH) | 80.6 |
| 3 (CH) | 119.9 |
| 4 (C) | 145 |
| 5 (CH2) | 40.7 |
| 6 (CH2) | 27.3 |
| 7 (CH) | 145.1 |
| 8 (C) | 131.6 |
| 9 (CH2) | 36.5 |
| 10 (CH2) | 25.9 |
| 11 (CH) | 124 |
| 12 (C) | 136 |
| 13 (CH2) | 37.2 |
| 14 (CH2) | 27.9 |
| 15 (CH) | 40.1 |
| 16 (C) | 178.9 |
| 17 (CH2) | 57.9 |
| 18 (CH3) | 15.1 |
| 19 (C) | 171 |
| 20 (CH3) | 16.2 |
| 17a (CH3) | 42.6 |
| 17b (CH3) | 45.7 |
