Spektraris NMR
Michaolides H
Common Name: Michaolides H
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C27H38O10/c1-14-8-10-20(33-16(3)28)15(2)9-11-22(35-18(5)30)27(6)25(37-27)24-23(21(12-14)34-17(4)29)19(13-32-7)26(31)36-24/h8-9,19-25H,10-13H2,1-7H3/b14-8+,15-9+/t19-,20-,21+,22+,23+,24-,25+,27-/m0/s1
InChIKey: InChIKey=OCEBYVKMYIOKNW-FCMIGLRISA-N
Formula: C27H38O10
Molecular Weight: 522.585667
Exact Mass: 522.246497
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Wang, L.T., Wang, S.K., Soong, K., Duh, C.Y. Chem Pharm Bull (2007) 55, 766-70
Species:
Notes: Family : Terpenoids, Type : Diterpenoids, Group : Cembranes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH) | 39.9 |
| 2 (CH) | 74.6 |
| 3 (CH) | 62.3 |
| 4 (C) | 62.6 |
| 5 (CH) | 77.8 |
| 6 (CH2) | 30.3 |
| 7 (CH) | 122 |
| 8 (C) | 135.9 |
| 9 (CH) | 78.5 |
| 10 (CH2) | 29.8 |
| 11 (CH) | 123.6 |
| 12 (C) | 133 |
| 13 (CH2) | 41.9 |
| 14 (CH) | 70.9 |
| 15 (CH) | 44 |
| 16 (CH2) | 69.3 |
| 17 (C) | 175.4 |
| 18 (CH3) | 13.7 |
| 19 (CH3) | 11.2 |
| 20 (CH3) | 15.7 |
| 5a (C) | 170.1 |
| 5b (CH3) | 21.2 |
| 9a (C) | 170.3 |
| 9b (CH3) | 21.3 |
| 14a (C) | 170.5 |
| 14b (CH3) | 21.4 |
| 16a (CH3) | 59.2 |
