Spektraris NMR
8b -Hydroxy-teucrolivin B
Common Name: 8b -Hydroxy-teucrolivin B
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C24H32O10/c1-14(25)32-12-22-19(28)18(27)21(4,29)20(3,8-5-16-7-10-31-11-16)24(22,30)9-6-17(34-15(2)26)23(22)13-33-23/h7,10-11,17,19,28-30H,5-6,8-9,12-13H2,1-4H3/t17-,19-,20-,21-,22-,23+,24-/m0/s1
InChIKey: InChIKey=AHBOQICKWFLQLC-PQURANIKSA-N
Formula: C24H32O10
Molecular Weight: 480.505815
Exact Mass: 480.199547
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Bruno, M., Rosselli, S., Maggio, A., Piozzi, F., Scaglioni, L., Arnold, N.A., Simmonds, M.S. Chem Pharm Bull (2004) 52, 1497-500
Species:
Notes: Family : Terpenoids, Type : Diterpenoids, Group : Clerodanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 27.45 |
| 2 (CH2) | 25.09 |
| 3 (CH) | 66.3 |
| 4 (C) | 61.29 |
| 5 (C) | 55.53 |
| 6 (CH) | 71.54 |
| 7 (C) | 208.56 |
| 8 (C) | 84.33 |
| 9 (C) | 49.58 |
| 10 (C) | 82.27 |
| 11 (CH2) | 31.31 |
| 12 (CH2) | 22.31 |
| 13 (C) | 124.98 |
| 14 (CH) | 110.74 |
| 15 (CH) | 142.9 |
| 16 (CH) | 138.56 |
| 17 (CH3) | 17.04 |
| 18 (CH2) | 46.1 |
| 19 (CH2) | 63.26 |
| 20 (CH3) | 19 |
| 3a (C) | 171.15 |
| 3b (CH3) | 20.85 |
| 19a (C) | 169.74 |
| 19b (CH3) | 20.95 |
