Spektraris NMR
8,17-Epoxy-14,15-dinor-labdan-13-one
Common Name: 8,17-Epoxy-14,15-dinor-labdan-13-one
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C18H30O2/c1-13(19)6-7-15-17(4)10-5-9-16(2,3)14(17)8-11-18(15)12-20-18/h14-15H,5-12H2,1-4H3/t14-,15+,17-,18-/m0/s1
InChIKey: InChIKey=GXWSUAHVPGIWCI-MVJTYMMSSA-N
Formula: C18H30O2
Molecular Weight: 278.430279
Exact Mass: 278.22458
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Basabe, P., Bodero, O., Marcos, I.S., Diez, D., Roman, M.d., Bianco, A., Urones, J.G. Tetrahedron (2007) 63, 11838-43
Species:
Notes: Family : Terpenoids, Type : Diterpenoids, Group : Labdanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 39.2 |
| 2 (CH2) | 18.9 |
| 3 (CH2) | 42.1 |
| 4 (C) | 33.6 |
| 5 (CH) | 53.4 |
| 6 (CH2) | 22 |
| 7 (CH2) | 36.8 |
| 8 (C) | 59.7 |
| 9 (CH) | 55.2 |
| 10 (C) | 40.5 |
| 11 (CH2) | 16.2 |
| 12 (CH2) | 45.4 |
| 13 (C) | 209.6 |
| 16 (CH3) | 30.1 |
| 17 (CH2) | 42.1 |
| 18 (CH3) | 33.6 |
| 19 (CH3) | 21.9 |
| 20 (CH3) | 14.7 |
