Spektraris NMR
14,15-Bisnor-8-hydroxylabd-11-en-13-one
Common Name: 14,15-Bisnor-8-hydroxylabd-11-en-13-one
Synonyms: 14,15-Bisnor-8-hydroxylabd-11-en-13-one
CAS Registry Number:
InChI: InChI=1S/C18H30O2/c1-13(19)7-8-15-17(4)11-6-10-16(2,3)14(17)9-12-18(15,5)20/h7-8,14-15,20H,6,9-12H2,1-5H3/b8-7+/t14-,15+,17-,18+/m0/s1
InChIKey: InChIKey=SNUHZNCSBAQVJV-JIDYTCFASA-N
Formula: C18H30O2
Molecular Weight: 278.430279
Exact Mass: 278.22458
NMR Solvent: CD3OD
MHz:
Calibration:
NMR references: 13C - Yang, X.W., Li, S.M., Feng, L., Shen, Y.H., Tian, J.M., Liu, X.H., Zeng, H.W., Zhang, C., Zhang, W.D. Tetrahedron (2008) 64, 4354-62
Species:
Notes: Family : Terpenoids, Type : Diterpenoids, Group : Labdanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 42.2 |
| 2 (CH2) | 19.4 |
| 3 (CH2) | 43 |
| 4 (C) | 33.9 |
| 5 (CH) | 56.9 |
| 6 (CH2) | 21.3 |
| 7 (CH2) | 44.8 |
| 8 (C) | 73.5 |
| 9 (CH) | 67 |
| 10 (C) | 39.2 |
| 11 (CH) | 147.8 |
| 12 (CH) | 136.5 |
| 13 (C) | 201.1 |
| 14 (CH3) | 27.1 |
| 17 (CH3) | 24.3 |
| 18 (CH3) | 34.3 |
| 19 (CH3) | 22 |
| 20 (CH3) | 16.6 |
