Spektraris NMR
Campylopin
Common Name: Campylopin
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C22H28O5/c1-11-13-7-14-19(26)21-6-4-5-20(3,10-23)15(21)9-17(27-12(2)24)22(14,18(11)25)16(21)8-13/h10,13-18,25H,1,4-9H2,2-3H3/t13-,14?,15+,16-,17+,18-,20-,21-,22+/m0/s1
InChIKey: InChIKey=ZDNMDOAXDDWWQL-BRUFKETFSA-N
Formula: C22H28O5
Molecular Weight: 372.455555
Exact Mass: 372.193674
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Wang, F.P., Yan, L.P. Tetrahedron (2007) 63, 1417-20
Species:
Notes: Family : Terpenoids, Type : Diterpenoids, Group : Hetidanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 28.9 |
| 2 (CH2) | 19.1 |
| 3 (CH2) | 35.3 |
| 4 (C) | 48.2 |
| 5 (CH) | 49.1 |
| 6 (CH2) | 27.3 |
| 7 (CH) | 71.4 |
| 8 (C) | 47.5 |
| 9 (CH) | 47.3 |
| 10 (C) | 52.3 |
| 11 (CH2) | 27.5 |
| 12 (CH) | 34.5 |
| 13 (CH2) | 32.2 |
| 14 (CH) | 45 |
| 15 (CH) | 65.7 |
| 16 (C) | 153.4 |
| 17 (CH2) | 108 |
| 18 (CH3) | 24 |
| 19 (CH) | 205.5 |
| 20 (C) | 224.6 |
| 7a (C) | 171.7 |
| 7b (CH3) | 21.1 |
