Spektraris NMR
Granaxylocarpins B
Common Name: Granaxylocarpins B
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C32H38O10/c1-8-17(2)29(37)42-28(20-15-30(4,5)21(13-24(34)39-7)18(3)26(20)36)32(38)22-14-25(35)41-27(19-10-12-40-16-19)31(22,6)11-9-23(32)33/h8,10,12,14-16,18,21,27-28,38H,9,11,13H2,1-7H3/b17-8+/t18-,21-,27+,28-,31-,32+/m1/s1
InChIKey: InChIKey=ZBJPDPDKXYNWFV-PQAYMIJJSA-N
Formula: C32H38O10
Molecular Weight: 582.639347
Exact Mass: 582.246497
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Yin, S., Wang, X.N., Fan, C.Q., Lin, L.P., Ding, J., Yue, J.M. J Nat Prod (2007) 70, 682-5
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Limonoids; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (C) | 198.7 |
| 2 (C) | 128.8 |
| 3 (CH) | 161.8 |
| 4 (C) | 36.8 |
| 5 (CH) | 45.2 |
| 6 (CH2) | 34.6 |
| 7 (C) | 173.4 |
| 8 (C) | 80.2 |
| 9 (C) | 208.8 |
| 10 (CH) | 42.8 |
| 11 (CH2) | 33 |
| 12 (CH2) | 25.5 |
| 13 (C) | 38.3 |
| 14 (C) | 163.5 |
| 15 (CH) | 118.4 |
| 16 (C) | 163.3 |
| 17 (CH) | 80 |
| 18 (CH3) | 18.5 |
| 19 (CH3) | 11.5 |
| 20 (C) | 119.6 |
| 21 (CH) | 141.4 |
| 22 (CH) | 109.8 |
| 23 (CH) | 143.3 |
| 28 (CH3) | 27.8 |
| 29 (CH3) | 20.5 |
| 30 (CH) | 67.5 |
| 7a (CH3) | 52 |
| 30a (C) | 166.8 |
| 30b (C) | 127.7 |
| 30c (CH) | 139.9 |
| 30d (CH3) | 14.7 |
| 30ba (CH3) | 12.1 |
