Spektraris NMR
Ganoderic acid AP2
Common Name: Ganoderic acid AP2
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C34H50O8/c1-18(11-10-12-19(2)30(39)40)23-17-26(41-20(3)35)33(8)22-13-14-24-31(5,6)25(37)15-16-32(24,7)27(22)28(38)29(34(23,33)9)42-21(4)36/h12,18,23-26,29,37H,10-11,13-17H2,1-9H3,(H,39,40)/b19-12+/t18-,23-,24+,25+,26+,29-,32+,33-,34+/m1/s1
InChIKey: InChIKey=QLPXRZYNNFETED-TZTJHZGXSA-N
Formula: C34H50O8
Molecular Weight: 586.757298
Exact Mass: 586.350569
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Wang, F., Liu, J.K. Chem Pharm Bull (2008) 56, 1035-7
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Lanostanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 33.8 |
| 2 (CH2) | 27.5 |
| 3 (CH) | 78.5 |
| 4 (C) | 38.8 |
| 5 (CH) | 51.3 |
| 6 (CH2) | 17.3 |
| 7 (CH2) | 29.3 |
| 8 (C) | 161.5 |
| 9 (C) | 140.1 |
| 10 (C) | 37.5 |
| 11 (C) | 191.6 |
| 12 (CH) | 80.1 |
| 13 (C) | 51.5 |
| 14 (C) | 53.9 |
| 15 (CH) | 74.6 |
| 16 (CH2) | 33.6 |
| 17 (CH) | 48.6 |
| 18 (CH3) | 12.3 |
| 19 (CH3) | 19 |
| 20 (CH) | 34.1 |
| 21 (CH3) | 19.7 |
| 22 (CH2) | 33.7 |
| 23 (CH2) | 26.3 |
| 24 (CH) | 144.2 |
| 25 (C) | 127.2 |
| 26 (C) | 172.7 |
| 27 (CH3) | 12 |
| 28 (CH3) | 28.2 |
| 29 (CH3) | 15.7 |
| 30 (CH3) | 19.8 |
| 12a (C) | 170.5 |
| 12b (CH3) | 21 |
| 15a (C) | 170.6 |
| 15b (CH3) | 21.3 |
