Spektraris NMR
Eryloside V
Common Name: Eryloside V
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C48H80O17/c1-23(12-18-47(9,59)43(2,3)4)24-14-19-48(42(57)58)26-10-11-30-44(5,6)31(15-16-45(30,7)25(26)13-17-46(24,48)8)63-41-38(65-40-36(56)34(54)33(53)29(20-49)62-40)37(28(51)22-61-41)64-39-35(55)32(52)27(50)21-60-39/h23-24,27-41,49-56,59H,10-22H2,1-9H3,(H,57,58)/t23-,24-,27-,28+,29-,30+,31+,32+,33+,34+,35-,36-,37+,38-,39+,40+,41+,45-,46-,47?,48+/m1/s1
InChIKey: InChIKey=LBXIYXJRXVQHDD-YXZLRKIQSA-N
Formula: C48H80O17
Molecular Weight: 929.140467
Exact Mass: 928.539551
NMR Solvent: C5D5N
MHz:
Calibration:
NMR references: 13C - Afiyatullov, S.S., Kalinovsky, A.I., Antonov, A.S., Ponomarenko, L.P., Dmitrenok, P.S., Aminin, D.L., Krasokhin, V.B., Nosova, V.M., Kisin, A.V. J Nat Prod (2007) 70, 1871-7
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Lanostanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 35.3 |
| 2 (CH2) | 27 |
| 3 (CH) | 88.4 |
| 4 (C) | 39.6 |
| 5 (CH) | 50.2 |
| 6 (CH2) | 18.4 |
| 7 (CH2) | 27.9 |
| 8 (C) | 127.9 |
| 9 (C) | 139.9 |
| 10 (C) | 37.3 |
| 11 (CH2) | 22.5 |
| 12 (CH2) | 31.7 |
| 13 (C) | 46.9 |
| 14 (C) | 62.8 |
| 15 (CH2) | 28.3 |
| 16 (CH2) | 29.5 |
| 17 (CH) | 51.6 |
| 18 (CH3) | 18 |
| 19 (CH3) | 19.6 |
| 20 (CH) | 37.3 |
| 21 (CH3) | 18.8 |
| 22 (CH2) | 30.3 |
| 23 (CH2) | 33.4 |
| 24 (C) | 75.3 |
| 25 (C) | 38.5 |
| 26 (CH3) | 25.7 |
| 27 (CH3) | 25.7 |
| 28 (CH3) | 27.4 |
| 29 (CH3) | 16.4 |
| 30 (C) | 178.3 |
| 1' (CH) | 105 |
| 2' (CH) | 77.4 |
| 3' (CH) | 82.2 |
| 4' (CH) | 68.5 |
| 5' (CH2) | 65.4 |
| 1'' (CH) | 105.1 |
| 2'' (CH) | 74.8 |
| 3'' (CH) | 78 |
| 4'' (CH) | 70.7 |
| 5'' (CH) | 66.9 |
| 6'' (CH2) | 104.9 |
| 1''' (CH) | 73.3 |
| 2''' (CH) | 75.2 |
| 3''' (CH) | 69.4 |
| 4''' (CH) | 76.1 |
| 5''' (CH2) | 61.1 |
| 24a (CH3) | 20.9 |
| 25a (CH3) | 25.7 |
