Spektraris NMR
(+)-Amphinolide W
Common Name: (+)-Amphinolide W
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C24H38O4/c1-6-7-10-17(2)15-18(3)16-22(26)23-12-9-8-11-19(4)21(25)14-13-20(5)24(27)28-23/h7,9-10,12,15,18-20,22-23,26H,6,8,11,13-14,16H2,1-5H3/b10-7+,12-9+,17-15+/t18-,19+,20-,22-,23-/m0/s1
InChIKey: InChIKey=VWINOFLMOJPXGV-UMSNSZKISA-N
Formula: C24H38O4
Molecular Weight: 390.55703
Exact Mass: 390.27701
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Ghosh, A.K., Gong, G. J Org Chem (2006) 71, 1085-93
Species:
Notes: Family : Polyketides, Type : Macrolides, Group : Amphidinolides; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (C) | 175.3 |
| 2 (CH) | 39.3 |
| 3 (CH2) | 25.8 |
| 4 (CH2) | 35.9 |
| 5 (C) | 212.8 |
| 6 (CH) | 45.8 |
| 7 (CH2) | 32.3 |
| 8 (CH2) | 32.3 |
| 9 (CH) | 138.2 |
| 10 (CH) | 127.2 |
| 11 (CH) | 79 |
| 12 (CH) | 70.6 |
| 13 (CH2) | 41 |
| 14 (CH) | 28.8 |
| 15 (CH) | 135.5 |
| 16 (C) | 133.5 |
| 17 (CH) | 133.7 |
| 18 (CH) | 129.8 |
| 19 (CH2) | 26.5 |
| 20 (CH3) | 13.8 |
| 21 (CH3) | 16.4 |
| 22 (CH3) | 18.6 |
| 23 (CH3) | 21.7 |
| 24 (CH3) | 12.7 |
