Spektraris NMR
3b-Hydroxyolean-(28,13)-olide
Common Name: 3b-Hydroxyolean-(28,13)-olide
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C30H48O3/c1-24(2)14-16-29-17-15-28(7)27(6)12-8-19-25(3,4)22(31)10-11-26(19,5)20(27)9-13-30(28,21(29)18-24)33-23(29)32/h19-22,31H,8-18H2,1-7H3/t19-,20+,21+,22-,26-,27+,28-,29-,30-/m0/s1
InChIKey: InChIKey=HESDPPFWDULRQU-LZRJWOMQSA-N
Formula: C30H48O3
Molecular Weight: 456.701448
Exact Mass: 456.360345
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Katai M., Terai T., Meguri H. Chem Pharm Bull (1983) 31, 1567
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Oleananes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 38.8 |
| 2 (CH2) | 27.3 |
| 3 (CH) | 78.8 |
| 4 (C) | 38.8 |
| 5 (CH) | 55 |
| 6 (CH2) | 17.7 |
| 7 (CH2) | 34.5 |
| 8 (C) | 42.2 |
| 9 (CH) | 50.6 |
| 10 (C) | 36.8 |
| 11 (CH2) | 19.6 |
| 12 (CH2) | 27.3 |
| 13 (C) | 91.7 |
| 14 (C) | 42.2 |
| 15 (CH2) | 28.6 |
| 16 (CH2) | 20.8 |
| 17 (C) | 44 |
| 18 (CH) | 50.4 |
| 19 (CH2) | 37.4 |
| 20 (C) | 31.5 |
| 21 (CH2) | 33.5 |
| 22 (CH2) | 31.4 |
| 23 (CH3) | 28 |
| 24 (CH3) | 15.2 |
| 25 (CH3) | 15.9 |
| 26 (CH3) | 18.3 |
| 27 (CH3) | 18.1 |
| 28 (C) | 180.3 |
| 29 (CH3) | 23.8 |
| 30 (CH3) | 23.8 |
