Spektraris NMR
Galphin A
Common Name: Galphin A
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C34H48O10/c1-18-9-10-29(5)11-13-31(7)25-22(43-21(4)36)16-32(17-41-20(3)35)19(2)42-27(37)24-23(44-24)26(32)30(25,6)12-14-33(31,28(38)40-8)34(29,39)15-18/h19,22-26,39H,1,9-17H2,2-8H3/t19-,22-,23-,24+,25+,26+,29-,30-,31-,32+,33+,34+/m1/s1
InChIKey: InChIKey=BORSFZZOEWEFDW-GIYHTGANSA-N
Formula: C34H48O10
Molecular Weight: 616.740226
Exact Mass: 616.324748
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - del Rayo Camacho, M., Phillipson, J.D., Croft, S.L., Marley, D., Kirby, G.C., Warhurst, D.C. J Nat Prod (2002) 65, 1457-61
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Friedelanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH) | 52.7 |
| 2 (CH) | 56.4 |
| 3 (C) | 168.6 |
| 4 (CH) | 76.3 |
| 5 (C) | 41.1 |
| 6 (CH2) | 31.8 |
| 7 (CH) | 69 |
| 8 (CH) | 50.4 |
| 9 (C) | 37.9 |
| 10 (CH) | 53.8 |
| 11 (CH2) | 27.1 |
| 12 (CH2) | 33.9 |
| 13 (C) | 57.1 |
| 14 (C) | 42.1 |
| 15 (CH2) | 40.4 |
| 16 (CH2) | 23.4 |
| 17 (C) | 38.2 |
| 18 (C) | 77 |
| 19 (CH2) | 42.6 |
| 20 (C) | 144.2 |
| 21 (CH2) | 29.1 |
| 22 (CH2) | 36.1 |
| 23 (CH3) | 13 |
| 24 (CH2) | 68.2 |
| 25 (CH3) | 22.7 |
| 26 (CH3) | 20.5 |
| 27 (C) | 174.6 |
| 28 (CH3) | 25.7 |
| 29 (CH2) | 109.7 |
| 7a (C) | 170.2 |
| 7b (CH3) | 21 |
| 24a (C) | 170.9 |
| 24b (CH3) | 21.6 |
| 27a (CH3) | 51.3 |
