Spektraris NMR
Galphimidin
Common Name: Galphimidin
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C34H52O10/c1-18-15-22(28(39)42-8)30(6)12-13-31(7)26-25(37)27(38)32(17-43-20(3)35)19(2)23(44-21(4)36)9-10-24(32)29(26,5)11-14-33(31,40)34(30,41)16-18/h19,22-27,37-38,40-41H,1,9-17H2,2-8H3/t19-,22+,23-,24-,25-,26-,27+,29-,30-,31+,32+,33-,34-/m0/s1
InChIKey: InChIKey=LEPHNIMCHVHFLZ-SMDOXGPFSA-N
Formula: C34H52O10
Molecular Weight: 620.771989
Exact Mass: 620.356048
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - del Rayo Camacho, M., Phillipson, J.D., Croft, S.L., Marley, D., Kirby, G.C., Warhurst, D.C. J Nat Prod (2002) 65, 1457-61
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Friedelanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 16.2 |
| 2 (CH2) | 31.5 |
| 3 (CH) | 74.7 |
| 4 (CH) | 49.1 |
| 5 (C) | 45.4 |
| 6 (CH) | 86.3 |
| 7 (CH) | 72.5 |
| 8 (CH) | 50 |
| 9 (C) | 37.5 |
| 10 (CH) | 59.3 |
| 11 (CH2) | 30.4 |
| 12 (CH2) | 29.6 |
| 13 (C) | 79.9 |
| 14 (C) | 43.8 |
| 15 (CH2) | 39.8 |
| 16 (CH2) | 25.3 |
| 17 (C) | 41.5 |
| 18 (C) | 79.5 |
| 19 (CH2) | 45 |
| 20 (C) | 144.1 |
| 21 (CH2) | 33.2 |
| 22 (CH) | 52.7 |
| 23 (CH3) | 16.7 |
| 24 (CH2) | 65.1 |
| 25 (CH3) | 23 |
| 26 (CH3) | 19.5 |
| 27 (C) | 174.8 |
| 28 (CH3) | 22.8 |
| 29 (CH2) | 110.4 |
| 3a (C) | 170 |
| 3b (CH3) | 21.4 |
| 24a (C) | 170.6 |
| 24b (CH3) | 21.2 |
| 27a (CH3) | 51.4 |
