Spektraris NMR
Carinoside C
Common Name: Carinoside C
Synonyms:
CAS Registry Number: 1702430-61-2
InChI:
InChIKey:
Formula: C56H62O29
Molecular Weight: 1199.083
Exact Mass: 1198.3377
NMR Solvent: DMSO-d6
MHz: 500 (1H), 125 (13C)
Calibration: TMS
NMR references: Bao, B., Wang, Q., Wu, X., Tai, W. (2015). The isolation and structural elucidation of three new biflavonoid glycosides from Lomatogonium carinthiacum. Nat. Prod. Res. 29, 1358-1362.
Species: Lomatogonium carinthiacum - Bao, B., Wang, Q., Wu, X., Tai, W. (2015). The isolation and structural elucidation of three new biflavonoid glycosides from Lomatogonium carinthiacum. Nat. Prod. Res. 29, 1358-1362.
Notes:
Proton NMR Peaks
| Position | PPM | Peak Type | J (Hz) |
|---|---|---|---|
| 3 | 6.86 | s | |
| 8 | 6.83 | s | |
| 11 | 4.58 | d | 9 |
| 2' | 7.97 | d | 7.5 |
| 3' | 6.94 | d | 7.5 |
| 5' | 6.94 | d | 7.5 |
| 6' | 7.97 | d | 7.5 |
| Araf-1 | 3.98 | dd | 10, 9 |
| Araf-2 | 3.2 | m | |
| Araf-3 | 3.09 | m | |
| Araf-4 | 3.33 | m | |
| Araf-5 | 3.99 | m | |
| Araf-5 | 3.42 | m | |
| Glc-1 | 4.13 | d | 6 |
| Glc-2 | 2.95 | m | |
| Glc-3 | 3.06 | m | |
| Glc-4 | 3.05 | m | |
| Glc-5 | 3.08 | m | |
| Glc-6 | 3.45 | m | |
| Glc-6 | 3.66 | m | |
| 7-OCH3 | 3.87 | s | |
| 3" | 6.86 | s | |
| 8" | 6.83 | s | |
| 11" | 4.57 | d | 9 |
| 2''' | 7.97 | d | 7.5 |
| 3''' | 6.94 | d | 7.5 |
| 5''' | 6.94 | d | 7.5 |
| 6''' | 7.97 | d | 7.5 |
| Araf-1' | 4.17 | dd | 10, 9 |
| Araf-2' | 3.19 | m | |
| Araf-3' | 3.08 | m | |
| Araf-4' | 3.32 | m | |
| Araf-5' | 4.01 | m | |
| Araf-5' | 3.43 | m | |
| Glc-1' | 4.13 | d | 6 |
| Glc-2' | 2.94 | m | |
| Glc-3' | 3.05 | m | |
| Glc-4' | 3.04 | m | |
| Glc-5' | 3.07 | m | |
| Glc-6' | 3.44 | m | |
| Glc-6' | 3.65 | m | |
| 7"-OCH3 | 3.89 | s |
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 2 | 164.4 |
| 3 | 103.6 |
| 4 | 182.7 |
| 5 | 160.7 |
| 6 | 110 |
| 7 | 165.4 |
| 8 | 91.7 |
| 9 | 157.3 |
| 10 | 105.1 |
| 11 | 73.4 |
| 1' | 121.4 |
| 2' | 129 |
| 3' | 116.5 |
| 4' | 161.9 |
| 5' | 116.5 |
| 6' | 129 |
| Araf-1 | 70.7 |
| Araf-2 | 79.4 |
| Araf-3 | 71.3 |
| Araf-4 | 80.5 |
| Araf-5 | 69.8 |
| Glc-1 | 103.5 |
| Glc-2 | 73.8 |
| Glc-3 | 77.2 |
| Glc-4 | 70.4 |
| Glc-5 | 77.3 |
| Glc-6 | 61.4 |
| 7-OCH3 | 56.8 |
| 2" | 164.1 |
| 3" | 103.6 |
| 4" | 182.4 |
| 5" | 159.9 |
| 6" | 110 |
| 7" | 164.2 |
| 8" | 90.7 |
| 9" | 157.2 |
| 10" | 104.6 |
| 11" | 73.1 |
| 1''' | 124.4 |
| 2''' | 129 |
| 3''' | 116.5 |
| 4''' | 161.8 |
| 5''' | 116.5 |
| 6''' | 129 |
| Araf-1' | 70 |
| Araf-2' | 79.3 |
| Araf-3' | 71.1 |
| Araf-4' | 80.3 |
| Araf-5' | 69.8 |
| Glc-1' | 103.5 |
| Glc-2' | 73.7 |
| Glc-3' | 77.2 |
| Glc-4' | 70.4 |
| Glc-5' | 77.3 |
| Glc-6' | 61.4 |
| 7"-OCH3 | 56.9 |
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The Spektraris NMR database is developed and hosted by the Lange laboratory at WSU. CAS Registry Number is a Registered Trademark of the American Chemical Society.