Spektraris NMR
Galphimine E
Common Name: Galphimine E
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C32H46O8/c1-19-10-11-27(4)12-14-29(6)23-16-24(40-21(3)34)30(20(2)33)18-39-25(35)9-8-22(30)28(23,5)13-15-31(29,26(36)38-7)32(27,37)17-19/h8-10,20,22-24,33,37H,11-18H2,1-7H3/t20?,22-,23-,24-,27+,28-,29+,30+,31-,32-/m0/s1
InChIKey: InChIKey=UXXPJNKPHVNPIM-VNARJOGMSA-N
Formula: C32H46O8
Molecular Weight: 558.704063
Exact Mass: 558.319268
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Cardoso Taketa, A.T., Lozada-Lechuga, J., Fragoso-Serrano, M., Villarreal, M.L., Pereda-Miranda, R. Phytochemistry (2004) 67, 644-9
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Friedelanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH) | 144.7 |
| 2 (CH) | 123.9 |
| 3 (C) | 169.3 |
| 4 (CH) | 63.8 |
| 5 (C) | 51.5 |
| 6 (CH) | 69.9 |
| 7 (CH2) | 65.3 |
| 8 (CH) | 52.7 |
| 9 (C) | 39.3 |
| 10 (CH) | 52 |
| 11 (CH2) | 40.4 |
| 12 (CH2) | 23.4 |
| 13 (C) | 57.6 |
| 14 (C) | 42.1 |
| 15 (CH2) | 29.2 |
| 16 (CH2) | 31.9 |
| 17 (C) | 37.1 |
| 18 (C) | 76.6 |
| 19 (CH2) | 40.2 |
| 20 (C) | 131.6 |
| 21 (CH) | 118.8 |
| 22 (CH2) | 38.7 |
| 23 (CH3) | 18 |
| 24 (CH2) | 69.4 |
| 25 (CH3) | 21.4 |
| 26 (CH3) | 21.7 |
| 27 (C) | 175.1 |
| 28 (CH3) | 26.6 |
| 29 (CH3) | 22.9 |
| 6a (C) | 169.7 |
| 6b (CH3) | 20.9 |
| 27a (CH3) | 51.3 |
