Spektraris NMR
Galphimine I
Common Name: Galphimine I
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C32H46O9/c1-18-10-11-27(4)12-14-29(6)24-23(41-20(3)34)25(36)30(19(2)33)17-40-22(35)9-8-21(30)28(24,5)13-15-31(29,26(37)39-7)32(27,38)16-18/h8-9,19,21,23-25,33,36,38H,1,10-17H2,2-7H3/t19?,21-,23-,24-,25-,27+,28-,29+,30+,31-,32-/m0/s1
InChIKey: InChIKey=PLOHJRTXRRLBGH-UNWDUKARSA-N
Formula: C32H46O9
Molecular Weight: 574.703468
Exact Mass: 574.314183
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Cardoso Taketa, A.T., Lozada-Lechuga, J., Fragoso-Serrano, M., Villarreal, M.L., Pereda-Miranda, R. Phytochemistry (2004) 67, 644-9
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Friedelanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH) | 144.4 |
| 2 (CH) | 123.8 |
| 3 (C) | 169.6 |
| 4 (CH) | 64.4 |
| 5 (C) | 52.1 |
| 6 (CH) | 65.4 |
| 7 (CH) | 70.9 |
| 8 (CH) | 50.1 |
| 9 (C) | 38.8 |
| 10 (CH) | 53.5 |
| 11 (CH2) | 40.6 |
| 12 (CH2) | 23.3 |
| 13 (C) | 57.4 |
| 14 (C) | 42.2 |
| 15 (CH2) | 27.4 |
| 16 (CH2) | 34.1 |
| 17 (C) | 38.1 |
| 18 (C) | 76.6 |
| 19 (CH2) | 42.5 |
| 20 (C) | 144.8 |
| 21 (CH2) | 28.9 |
| 22 (CH2) | 36 |
| 23 (CH3) | 18.2 |
| 24 (CH2) | 69.4 |
| 25 (CH3) | 22 |
| 26 (CH3) | 20.9 |
| 27 (C) | 175 |
| 28 (CH3) | 25.5 |
| 29 (CH2) | 109.4 |
| 7a (C) | 171.7 |
| 7b (CH3) | 21.6 |
| 27a (CH3) | 51.4 |
