Spektraris NMR
(3β,24)-3-Methoxy-24-methyl-9,19-cyclolanostan-25-ol
Common Name: (3β,24)-3-Methoxy-24-methyl-9,19-cyclolanostan-25-ol
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C32H56O2/c1-21(10-11-22(2)28(5,6)33)23-14-16-30(8)25-13-12-24-27(3,4)26(34-9)15-17-31(24)20-32(25,31)19-18-29(23,30)7/h21-26,33H,10-20H2,1-9H3/t21-,22?,23+,24+,25+,26+,29-,30+,31-,32+/m1/s1
InChIKey: InChIKey=YPJRQXJFROEIKW-QWKZLORGSA-N
Formula: C32H56O2
Molecular Weight: 472.787041
Exact Mass: 472.428031
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Su, H.J., Wang, L.W., Lin, C.N., Day, S.H., Wei, B.L., Yang, S.Z., Won, S.J. Helv Chim Acta (2003) 86, 2645-52
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Cycloartanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 31.8 |
| 2 (CH2) | 25.4 |
| 3 (CH) | 88.5 |
| 4 (C) | 40.5 |
| 5 (CH) | 47.7 |
| 6 (CH2) | 21 |
| 7 (CH2) | 28.1 |
| 8 (CH) | 48 |
| 9 (C) | 20 |
| 10 (C) | 26.3 |
| 11 (CH2) | 26 |
| 12 (CH2) | 32.9 |
| 13 (C) | 45 |
| 14 (C) | 48.8 |
| 15 (CH2) | 35.5 |
| 16 (CH2) | 26.5 |
| 17 (CH) | 52.2 |
| 18 (CH3) | 18 |
| 19 (CH2) | 29.8 |
| 20 (CH) | 36.7 |
| 21 (CH3) | 18.6 |
| 22 (CH2) | 35.2 |
| 23 (CH2) | 28.4 |
| 24 (CH) | 45.2 |
| 25 (C) | 73.6 |
| 26 (CH3) | 26.2 |
| 27 (CH3) | 27.1 |
| 28 (CH3) | 25.5 |
| 29 (CH3) | 14.8 |
| 30 (CH3) | 19.3 |
| 3a (CH3) | 57.6 |
| 24a (CH3) | 14.8 |
