Spektraris NMR
Beesioside L
Common Name: Beesioside L
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C37H58O10/c1-20(38)45-22-16-32(6)24-9-8-23-30(2,3)25(46-29-27(41)26(40)21(39)17-43-29)10-11-34(23)18-35(24,34)13-14-36(32)19-44-37(31(4,5)42)15-12-33(7,47-37)28(22)36/h21-29,39-42H,8-19H2,1-7H3/t21-,22+,23+,24+,25+,26+,27-,28+,29+,32+,33+,34-,35+,36+,37+/m1/s1
InChIKey: InChIKey=UFCGPJWMJBSBEB-BALGXZJDSA-N
Formula: C37H58O10
Molecular Weight: 662.851841
Exact Mass: 662.402998
NMR Solvent: C5D5N
MHz:
Calibration:
NMR references: 13C - Ju, J.H., Liu, D., Lin, G., Zhang, Y.M., Yang, J.S., Lu, Y., Gong, N.B., Zheng, Q.T. J Nat Prod (2002) 65, 147-52
Species:
Notes: Family : Terpenoids, Type : Triterpenoids, Group : Cycloartanes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (CH2) | 32.1 |
| 2 (CH2) | 30.9 |
| 3 (CH) | 88.3 |
| 4 (C) | 41.3 |
| 5 (CH) | 47.4 |
| 6 (CH2) | 20.5 |
| 7 (CH2) | 26.5 |
| 8 (CH) | 46.9 |
| 9 (C) | 18.9 |
| 10 (C) | 27.5 |
| 11 (CH2) | 26.5 |
| 12 (CH2) | 28.3 |
| 13 (C) | 44.3 |
| 14 (C) | 52.6 |
| 15 (CH2) | 43 |
| 16 (CH) | 73.2 |
| 17 (CH) | 59.3 |
| 18 (CH2) | 66.7 |
| 19 (CH2) | 31.1 |
| 20 (C) | 87.2 |
| 21 (CH3) | 32.6 |
| 22 (CH2) | 37.8 |
| 23 (CH2) | 30 |
| 24 (C) | 114.1 |
| 25 (C) | 72.8 |
| 26 (CH3) | 25.7 |
| 27 (CH3) | 25.7 |
| 28 (CH3) | 25.8 |
| 29 (CH3) | 15.4 |
| 30 (CH3) | 22.2 |
| 1' (CH) | 107.6 |
| 2' (CH) | 75.6 |
| 3' (CH) | 78.6 |
| 4' (CH) | 71.2 |
| 5' (CH2) | 67.1 |
| 16a (C) | 170.3 |
| 16b (CH3) | 21.4 |
