Spektraris NMR
Milolide B
Common Name: Milolide B
Synonyms:
CAS Registry Number:
InChI: InChI=1S/C24H34O9/c1-11-7-8-15(30-13(3)25)22(5)16(31-14(4)26)10-17-23(6,33-17)19(22)20(27)24(29)12(2)21(28)32-18(24)9-11/h9,12,15-20,27,29H,7-8,10H2,1-6H3/b11-9-/t12-,15-,16-,17-,18-,19+,20-,22-,23-,24-/m0/s1
InChIKey: InChIKey=QGRHFZHVNPHIGN-STTRNAQRSA-N
Formula: C24H34O9
Molecular Weight: 466.522292
Exact Mass: 466.220283
NMR Solvent: CDCl3
MHz:
Calibration:
NMR references: 13C - Kwak, J.H., Schmitz, F.J., Williams, G.C. J Nat Prod (2001) 64, 754-60
Species:
Notes: Family : Terpenoids, Type : Diterpenoids, Group : Briaranes; 13 C Spectrum from Naproc 13: José Luis López-Pérez, Roberto Therón, Esther del Olmo, David Díaz: NAPROC-13: a database for the dereplication of natural product mixtures in bioassay-guided protocols. Bioinformatics 23(23):3256-3257 (2007)
Carbon NMR Peaks
| Position | PPM |
|---|---|
| 1 (C) | 45.4 |
| 2 (CH) | 75.7 |
| 3 (CH2) | 31.9 |
| 4 (CH2) | 28.7 |
| 5 (C) | 146.9 |
| 6 (CH) | 117.7 |
| 7 (CH) | 78.4 |
| 8 (C) | 82.8 |
| 9 (CH) | 73.1 |
| 10 (CH) | 39.2 |
| 11 (C) | 65.2 |
| 12 (CH) | 61.1 |
| 13 (CH2) | 25.4 |
| 14 (CH) | 73.7 |
| 15 (CH3) | 15.5 |
| 16 (CH3) | 25.3 |
| 17 (CH) | 43.7 |
| 18 (CH3) | 6.9 |
| 19 (C) | 177.9 |
| 20 (CH3) | 25.3 |
| 2a (C) | 171 |
| 2b (CH3) | 21.4 |
| 14a (C) | 170.7 |
| 14b (CH3) | 21.2 |
